Smokeless tobacco lipid granules

ABSTRACT

A smokeless tobacco product includes a plurality of orally disintegrable granules. Each granule has a lipid core and at least one layer surrounding the core. The core can also include binders, powdered tobacco carbohydrates, water soluble polymers, flavorants, salts, sweeteners, and combinations thereof. The orally disintegrable granules can provide a pleasing texture and/or flavor experience.

CROSS-REFERENCE TO RELATED APPLICATIONS

This application is a divisional of U.S. application Ser. No.13/922,954, filed on Jun. 20, 2023, which claims priority to U.S.Provisional Application Ser. No. 61/662,060, filed on Jun. 20, 2012, thecontents of each of which are hereby incorporated by reference in theirentirety.

TECHNICAL FIELD

This disclosure relates to lipid granules and a method of producing thesame. The lipid granules can be used to form or to flavor smokelesstobacco products.

BACKGROUND

Smokeless tobacco is tobacco that is placed in the mouth and notcombusted. There are various types of smokeless tobacco including:chewing tobacco, moist smokeless tobacco, snus, and dry snuff. Chewingtobacco is coarsely divided tobacco leaf that is typically packaged in alarge pouch-like package and used in a plug or twist. Moist smokelesstobacco is a moist, more finely divided tobacco that is provided inloose form or in pouch form and is typically packaged in round cans andused as a pinch or in a pouch placed between an adult tobacco consumer'scheek and gum. Snus is a heat treated smokeless tobacco. Dry snuff isfinely ground tobacco that is placed in the mouth or used nasally.

SUMMARY

A smokeless tobacco product is described that includes a plurality oftobacco lipid granules. Each tobacco lipid granule has a core and atleast one layer surrounding the core. The core includes at least onelipid. Layers overlying the core can include tobacco particles,flavorants, carbohydrates, water soluble polymers, salts, sweeteners,binders, or combinations thereof. The lipid granules can exhibit variousflavor profiles and textures when used by an adult tobacco consumer.

The core includes a lipid. The lipid can be selected frommonoglycerides, diglycerides, triglycerides, and combinations thereof.In some embodiments, the lipid is a hydrogenated soybean oil. The corecan also include additional ingredients within a matrix of the lipid. Incertain embodiments, the core includes a mixture of lipid, binder, andflavorant. In some embodiments, one or more carbohydrates, water solublepolymers, flavorants, salts, sweeteners, or combinations thereof areincluded within a matrix of the lipid or a combination of lipid andbinder. In some embodiments, powdered tobacco is included in the corewithin a matrix of the lipid. The tobacco particles can have an averagediameter of less than 100 micrometers. The core can have a diameter ofgreater than 1 millimeter. In some embodiments, the core has a diameterof less than 5 millimeters. The core can have a diameter of between 1millimeter and 5 millimeters. In some embodiments, the core has adiameter of between 2 and 4 millimeters, between 2.5 and 3.5millimeters, or between 2.8 and 3.2 millimeters.

The granules include at least one layer overlying each core. The atleast one layer can include a binder, a flavorant, a carbohydrate, awater soluble polymer, a water insoluble polymer, a salt, a sweetener,tobacco powder, or a combination thereof. In some embodiments, thegranules include a plurality of layers overlying each core. Anadditional layer overlying the at least one layer and concentricallysurrounding the core includes a different composition than the at leastone layer. The additional layer can include a different composition thanthe at least one layer with regard to tobacco particle concentration,type of tobacco particles, binder, flavorant, or combination thereof. Insome embodiments, the additional layer has a different concentration oftobacco. In some embodiments, the layers have different flavorants.

A flavorant included in the core and/or one or more layers overlying thecore can be selected from the group consisting of licorice, wintergreen,cherry and berry type flavorants, Drambuie, bourbon, scotch, whiskey,spearmint, peppermint, lavender, cinnamon, cardamon, apium graveolens,clove, cascarilla, nutmeg, sandalwood, bergamot, geranium, honeyessence, rose oil, vanilla, lemon oil, orange oil, Japanese mint,cassia, caraway, cognac, jasmine, chamomile, menthol, ylang-ylang, sage,fennel, piment, ginger, anise, coriander, coffee, mint oils from aspecies of the genus Mentha, and combinations thereof. Tobacco extractscan also be added. For example, the tobacco extract can include two ormore tobacco organoleptic components.

Tobacco within the granules (either within the core or one or more ofthe layers) can be non-fermented tobacco. In some embodiments, eachgranule can include dry snuff. In some embodiments, each granuleincludes tobacco particles of cured tobacco prepared from plants havingless than 20 μg of DVT per cm² of green leaf tissue. In someembodiments, the tobacco is powdered tobacco. Powdered tobacco can beincorporated into a matrix of the lipid within the core and/orincorporated into one or more layers overlying the core. The tobaccoparticles of the powdered tobacco can have an average diameter of lessthan 100 micrometers.

The at least one layer and/or the core can include a binder. In someembodiments, the binder is selected from the group consisting ofcarboxymethyl cellulose, hydroxypropyl cellulose, hydroxyethylcellulose, hydroxypropyl methyl cellulose, methyl cellulose, konjac,collagen, inulin, soy protein, whey protein, casein, wheat gluten,carrageenan, alginates, propylene glycol alginate, xanthan, dextran,pullulan, curdlan, gellan, locust bean gum, guar gum, tara gum, gumtragacanth, pectin, agar, zein, karaya, gelatin, psyllium seed, chitin,chitosan, gum acacia, polyvinyl pyrrolidone, polyethylene oxide,polyvinyl alcohol, and combinations thereof. For example, the binder caninclude a hydroxyl containing compound and a dextrin or dextrinderivative.

The granules can be generally spherical. The total diameter of thegranules can have a diameter of between 1.1 millimeters and 6millimeters.

The tobacco particles can include a non-fermented tobacco. In someembodiments, the tobacco particles include dry snuff. In someembodiments, the tobacco particles are cured tobacco particles preparedfrom tobacco plants having less than 20 μg of DVT per cm² of green leaftissue. The tobacco particles in the at least one layer can have anaverage diameter of less than 100 micrometers.

The smokeless tobacco product can consist of a plurality of thegranules. In other embodiments, the smokeless tobacco product includesadditional components. For example, the smokeless tobacco product caninclude a pouch holding the plurality of granules. In some embodiments,the pouch can include an edible film. In some embodiments, the pouchincludes a plurality of pores. In some embodiments, the smokelesstobacco product includes loose smokeless tobacco having the plurality ofgranules dispersed within the loose smokeless tobacco. The loosesmokeless tobacco to granule ratio for the smokeless tobacco product canbe between 1:5 and 5:1 by weight.

The smokeless tobacco product can include a flavor profile having two ormore flavors each having a peak flavor intensity that is perceptible atdifferent times or concurrently during consumption. For example, eachgranule can provide a flavor profile. A plurality of granules within asmokeless tobacco product can provide the same or different flavorprofiles.

The lipid cores can be created by supplying a mixture including a lipidto a sphere forming machine. In some embodiments, the sphere formingmachine is a bead making machine. For example, the sphere formingmachine can be the Multi-Granulator, Model MC-55, or the BenchtopMarumerizer Model #QJ-230T-1, which are sold by Fuji Paudal Co. Ltd. Themixture can include a lipid and a binder. In some embodiments, themixture includes a flavorant, tobacco, a sweetener, and/or a solvent.The lipid cores can then be coated by fluidizing the lipid cores withina fluid bed processor having a rotor and spraying a binder solution orsuspension into the fluidized bed containing the fluidized cores. Insome embodiments, tobacco particles are also fed into the fluidized bed.The binding solution or suspension can include a flavorant. In someembodiments, the composition of the binder solution or suspension fedinto the fluidized bed is changed to create multiple layers.

The details of one or more embodiments are set forth in the accompanyingdrawings and the description below. Other features, objects, andadvantages will be apparent from the description and drawings, and fromthe claims.

DESCRIPTION OF DRAWINGS

FIGS. 1A-1D depict cross-sectional views of lipid granules according todifferent embodiments.

Like reference symbols in the various drawings indicate like elements.

DETAILED DESCRIPTION

This disclosure describes a smokeless tobacco product that includes aplurality of orally disintegrable granules 10. Examples of lipidgranules 10 are shown in FIGS. 1A-1D. Each granule has a core 12 and atleast one layer surrounding the core. The core 12 includes a lipid. Eachgranule can include more than one layer surrounding the lipid core.Thus, the present disclosure describes granules having differentarrangements, methods of making the granules, and smokeless tobaccoproducts including these granules. It has been discovered that granulesaccording to the instant disclosure can confer unique flavor profiles onsmokeless tobacco products.

The lipid core of the granules within a smokeless tobacco product canprovide an adult tobacco consumer with an improved tactile and flavorrelease experience. For example, the lipids can provide a favorablemouth coating sensation and a soft mouth feel. The coating or coatingsaround the lipid cores can reduce clustering of the lipid cores and/orprotect the lipid cores from deformation prior to use.

I. Cores

Cores 12 include at least one lipid. The lipid can be selected frommonoglycerides, diglycerides, triglycerides, and combinations thereof.In some embodiments, the lipid is a hydrogenated soybean oil. The core12 can have a diameter of greater than 1 millimeter. In someembodiments, the core 12 has a diameter of less than 5 millimeters.Cores 12 can have a diameter of between 1 millimeter and 5 millimeters.In some embodiments, the cores have a diameter of between 2 and 4millimeters, between 2.5 and 3.5 millimeters, or between 2.8 and 3.2millimeters.

The lipid core can include a binder. In some embodiments, the coreincludes between 5 and 70 weight percent lipid and between 30 and 95weight percent binder. For example, the lipid cores can include a ratioof lipid to binder of between 1:1 and 1:5. Binders suitable for use inthe core include orally compatible polymers, such as cellulosics (e.g.,microcrystalline cellulose (MCC), carboxymethyl cellulose (CMC),hydroxypropyl cellulose (HPC), hydroxyethyl cellulose (HEC),hydroxypropyl methyl cellulose (HPMC), and methyl cellulose (MC));natural polymers (e.g., starches and modified starches, konjac,collagen, inulin, soy protein, whey protein, casein, and wheat gluten);seaweed-derived polymers (e.g., carrageenan (kappa, iota, and lambda);alginates, (and propylene glycol alginate), microbial-derived polymers(e.g., xanthan, dextran, pullulan, curdlan, and gellan); extracts (e.g.,locust bean gum, guar gum, tara gum, gum tragacanth, pectin (lo methoxyand amidated), agar, zein, karaya, gelatin, psyllium seed, chitin, andchitosan), exudates (e.g., gum acacia (arabic) and shellac), syntheticpolymers (e.g., polyvinyl pyrrolidone, polyethylene oxide, and polyvinylalcohol)). Other useful binders are known in the art, for example, seeKrochta et al. Food Technology, 1997, 51:61-74; Glicksman FoodHydrocolloids CRC 1982; Krochta Edible Coatings and Films to ImproveFood Quality Technomic 1994; Industrial Gums Academic 1993; NussinovitchWater-Soluble Polymer Applications in Foods Blackwell Science 2003. Insome embodiments, the binder can include hydroxypropyl methyl cellulose,which can be obtained from the Dow Chemical Company under the tradenames HPMC E5, E15, and K4M.

The cores 12 can include other constituents, such as flavorants, salts,sweeteners, or tobacco particles. For example, a core can include one ormore sugars, such as glucose, lactose, or sucrose. Suitable saltsinclude citric acid salts and sodium chloride. In some embodiments, suchas shown in FIGS. 1A-1C, the core is tobacco free. In other embodiments,such as shown in FIG. 1D, the core includes tobacco particles dispersedwithin matrix of the lipid. In some embodiments, the core can includenon-tobacco additives and/or actives, such as caffeine. In someembodiments, the core comprises at least 50 weight percent lipids. Insome embodiments, the core can include less than 5 weight percent ofingredients other than lipid, tobacco, and flavorant.

The lipid cores 12 can be made by supplying a mixture of lipid, binder,and optionally tobacco particles, flavorants, and/or sweeteners to asphere forming machine. For example, the sphere forming machine can be abead making machine.

II. Layer(s)

Each granule 10 further includes at least one layer surrounding thelipid core 12. In some embodiments, as shown in FIGS. 1A and 1D, thegranule 10 can include a single layer surrounding the core 12. As shownin FIG. 1D, some embodiments of layer 14 include a binder and tobaccoparticles 22. In other embodiments, the granule 10 includes a pluralityof layers. FIG. 1B depicts an embodiment including two layers 15 and 16,with at least layer 15 including tobacco particles 22 and a binder.Layers 15 and 16 can differ in composition. For example, layers 15 and16 can differ in the type or concentration of tobacco particles, thetype of binder, and/or the type or concentration of flavorant. Otherembodiments can include three layers. For example, as shown in FIG. 1C,a first layer 19 and a second layer 18 can include tobacco particles anda binder, while a third layer 17 does not include tobacco. The first andsecond layers 18 and 19 can differ in the type or concentration oftobacco particles, the type of binder, and/or the type or concentrationof flavorant. The third layer 17 can include the same or a differentflavorant from the first and second layers. In some embodiments, one ormore of the layers can include other filler constituents, such as starchpowders. In other embodiments, not specifically shown, the granules 10can include any number of layers in which the layers can each have thesame or different constituents in different orders. For example, agranule could include six or more alternating layers in which everyother layer includes tobacco particles, each successive layer includes adifferent flavorant, and the binder varies between layers so differentlayers dissolve at different rates.

Binders

Binders suitable for use in the layers described herein include orallycompatible polymers, such as cellulosics (e.g., carboxymethyl cellulose(CMC), hydroxypropyl cellulose (HPC), hydroxyethyl cellulose (HEC),hydroxypropyl methyl cellulose (HPMC), and methyl cellulose (MC));natural polymers (e.g., starches and modified starches, konjac,collagen, inulin, soy protein, whey protein, casein, and wheat gluten);seaweed-derived polymers (e.g., carrageenan (kappa, iota, and lambda);alginates, (and propylene glycol alginate), microbial-derived polymers(e.g., xanthan, dextran, pullulan, curdlan, and gellan); extracts (e.g.,locust bean gum, guar gum, tara gum, gum tragacanth, pectin (lo methoxyand amidated), agar, zein, karaya, gelatin, psyllium seed, chitin, andchitosan), exudates (e.g., gum acacia (arabic) and shellac), syntheticpolymers (e.g., polyvinyl pyrrolidone, polyethylene oxide, and polyvinylalcohol)). Other useful binders are known in the art, for example, seeKrochta et al. Food Technology, 1997, 51:61-74; Glicksman FoodHydrocolloids CRC 1982; Krochta Edible Coatings and Films to ImproveFood Quality Technomic 1994; Industrial Gums Academic 1993; NussinovitchWater-Soluble Polymer Applications in Foods Blackwell Science 2003. Insome embodiments, the binder can include hydroxypropyl methyl cellulose,which can be obtained from the Dow Chemical Company under the tradenames HPMC ES, E15, and K4M.

Tobacco

One or more of the layers surrounding the core of a granule can containa plurality of tobacco particles 22. Core 12 can optionally includetobacco particles dispersed in the lipid. For example, FIG. 1D depictsan embodiment of a granule having tobacco particles dispersed in a lipidmatrix of the core 12. The average diameter of such tobacco particles istypically no more than ⅓ the size of the largest diameter of the core.In some embodiments, the average tobacco particle within a layer has anaverage diameter of no more than ⅕ the size of the average diameter ofthe core. For example, the core to tobacco particle average diameterratio can be less than 10:1, less than 50:1, or less than 100:1. Forexample, the tobacco particles can have an average diameter of less than200 micrometers (e.g., an average tobacco particle diameter of between10 micrometers and 40 micrometers, between 40 micrometers and 60micrometers, between 60 micrometers and 80 micrometers, between 80micrometers and 120 micrometers, between 120 micrometers and 160micrometers, or between 160 micrometers and 200 micrometers). In someembodiments, the average tobacco particle diameter is between 20micrometers and 40 micrometers (e.g., between 25 micrometers and 35micrometers). In some embodiments, the tobacco particles within the atleast one layer have an average diameter of less than 100 micrometers(e.g., about 80 micrometers). For example, the tobacco particles caninclude micronized tobacco powder. The tobacco particles can be sized ormade to disintegrate in the mouth (e.g., dissolve) or to give theperception of dissolvability (e.g., the tobacco does not produce atactile experience in the mouth). For example, a micronized tobaccopowder can have an average diameter of 27 micrometers and a ninety-ninthpercentile diameter of 120 micrometers. Alternatively, the tobacco maybe sized or made to provide a tactile experience in the mouth.

Depending on the desired characteristics, each layer can have a finaltobacco concentration ranging from 0 percent to 99 percent by weight(e.g., between 10 and 90 percent by weight, between 25 and 75 percent byweight, or between 40 and 60 percent by weight). For example, a layercan contain between 15 and 35 percent by weight tobacco (e.g., about 25percent by weight). In some embodiments, each granule within theplurality can include at least one layer including greater than 20percent tobacco (e.g., greater than 40 percent tobacco, greater than 60percent tobacco, or greater than 80 percent tobacco).

The tobacco used in the granule 10, either as the tobacco particles inthe layers and/or within the core, is a tobacco suitable for use insmokeless tobacco products. The tobacco is any tobacco suitable for usein the smokeless tobacco products. By “tobacco” it is meant a part,e.g., leaves, flowers, and stems, of a member of the genus Nicotiana.Exemplary species of tobacco include N. rustica, N. tabacum, N.tomentosiformis, and N. sylvestris. Suitable tobaccos include fermentedand unfermented tobaccos. In addition to fermentation, the tobacco canbe processed using other techniques. For example, tobacco can beprocessed by heat treatment (e.g., cooking, toasting), flavoring, enzymetreatment, expansion and/or curing. Both fermented and non-fermentedtobaccos can be processed using these techniques. In other embodiments,the tobacco can be unprocessed tobacco. Specific examples of suitableprocessed tobaccos include dark air-cured, dark fire-cured, burley, fluecured, and cigar filler or wrapper, as well as the products from thewhole leaf stemming operation. For example, tobacco can be conditionedby heating, sweating and/or pasteurizing steps as described in U.S.Publication Nos. 2004/0118422 or 2005/0178398. Fermenting is typicallycharacterized by high initial moisture content, heat generation, and a10 to 20% loss of dry weight. See e.g., U.S. Pat. Nos. 4,528,993;4,660,577; 4,848,373; and 5,372,149. In addition to modifying the aromaof the leaf, fermentation can change either or both the color andtexture of a leaf. Also during the fermentation process, evolution gasescan be produced, oxygen can be taken up, the pH can change, and theamount of water retained can change. See, for example, U.S. PublicationNo. 2005/0178398 and Tso (1999, Chapter 1 in Tobacco: Production,Chemistry and Technology, Davis & Nielsen, eds., Blackwell Publishing,Oxford). Cured, or cured and fermented tobacco can be further processed(e.g., cut, expanded, blended, milled or comminuted) prior toincorporation into the granules.

The tobacco can, in some embodiments, be prepared from plants havingless than 20 μg of DVT per cm² of green leaf tissue. For example, thetobacco particles can be selected from the tobaccos described in U.S.Patent Publication No. 2008/0209586, which is hereby incorporated byreference. Tobacco compositions containing tobacco from such low-DVTvarieties exhibit improved flavor characteristics in sensory panelevaluations when compared to tobacco or tobacco compositions that do nothave reduced levels of DVTs.

Flavorants

The cores and/or the one or more layers can include one or moreflavorants. Flavorants can produce a flavor release profile when thegranules 10 are orally consumed. The flavor release profile can becustomized by adjusting the ingredients and sizes of the layers. Forexample, by having a plurality of lipid granules each having the samepattern of layers, an adult tobacco consumer consuming the granules canidentify a flavor profile.

Flavorants used within the granules 10 can be any flavorant known in theart. For example, suitable flavorants include wintergreen, cherry andberry type flavorants, various liqueurs and liquors such as Drambuie,bourbon, scotch, whiskey, spearmint, peppermint, lavender, cinnamon,cardamon, apium graveolens, clove, cascarilla, nutmeg, sandalwood,bergamot, geranium, honey essence, rose oil, vanilla, lemon oil, orangeoil, Japanese mint, cassia, caraway, cognac, jasmine, chamomile,menthol, ylang-ylang, sage, fennel, piment, ginger, anise, coriander,coffee, and mint oils from a species of the genus Mentha. Mint oilsuseful in the granules include spearmint and peppermint.

Other Layer Constituents

Depending on the desired characteristics, layers or lipid cores may alsoinclude fillers (e.g., starch, di-calcium phosphate, lactose, sorbitol,mannitol, and microcrystalline cellulose), soluble fiber (e.g., Fibersolfrom Matsushita), calcium carbonate, dicalcium phosphate, calciumsulfate, and clays), lubricants (e.g., lecithin, stearic acid,hydrogenated vegetable oil, mineral oil, polyethylene glycol 4000-6000(PEG), sodium lauryl sulfate (SLS), glyceryl palmitostearate, sodiumbenzoate, sodium stearyl fumarate, talc, and stearates (e.g., Mg or K),and waxes (e.g., glycerol monostearate, propylene glycol monostearate,and acetylated monoglycerides)), plasticizers (e.g., glycerine,propylene glycol, polyethylene glycol, sorbitol, mannitol, triacetin,and 1,3 butane diol), stabilizers (e.g., ascorbic acid and monosterolcitrate, BHT, or BHA), artificial sweeteners (e.g., sucralose,saccharin, and aspartame), disintegrating agents (e.g., starch, sodiumstarch glycolate, cross caramellose, cross linked PVP), or othercompounds (e.g., vegetable oils, surfactants, and preservatives). Somecompounds display functional attributes that fall into more than one ofthese categories. For example, propylene glycol can act as both aplasticizer and a lubricant and sorbitol can act as both a filler and aplasticizer.

III. Smokeless Tobacco Products

A plurality of granules 10 can itself be a smokeless tobacco product orcan be incorporated with other materials into a smokeless tobaccoproduct. Smokeless tobacco compositions incorporating a plurality ofgranules 10 can contain, without limitation, moist or dry smokelesstobaccos including snus-style products, loose tobacco in a pouch or packor snuff tobaccos. See, e.g., U.S. Patent Publication Nos. 2005/0244521and 2006/0191548 for descriptions of a number of smokeless tobaccocompositions. Smokeless tobacco compositions having granules 10 mixedtherein can provide the smokeless tobacco composition with a desiredflavor release profile. The loose smokeless tobacco to granule ratio forthe smokeless tobacco product is not limited. In some embodiments, theloose smokeless tobacco to granule ratio is between 1 and 90weight/weight (wet). For example, the loose smokeless tobacco to granuleratio can be between 30 and 65 weight/weight (wet).

Granules 10 can also be packaged with other smokeless tobacco productswithout the granules 10 being intermixed with the other smokelesstobacco products. For example, granules 10 can be packaged along withother smokeless tobacco products in a divided container, with thegranules 10 in a different segment of the divided container. A dividedcontainer can allow an adult tobacco consumer to experience the granulesalone, the other smokeless tobacco product(s) alone, or a combination ofthe products together. A plurality of different types of granules 10could also be included in different sections of a divided container. Inother embodiments, the granules 10 are encapsulated in one or moreblisters inside the container of a smokeless tobacco product to allowfor an adult tobacco consumer selectively increase or alter the flavorof the smokeless tobacco product. For example, an adult tobacco consumercan have a moist smokeless tobacco product container with multipleblister packs inside the lid, each blister pack having granulesproviding a different flavor profile, and thus the adult tobaccoconsumer can elect a particular flavor or combination of flavors orelect to not use any flavors at all. Furthermore, granules can be addedto increase the flavor intensity after an initial use.

A plurality of the granules can, in some embodiments, be sold alone inpackages for direct oral consumption. For example, granules 10 can bepackaged loosely in sugar type paper packages, slide fastener plasticbags, blister packs, portion-control dispensers (e.g., like a peppergrinder), straws or tubes with sealed ends, and box-like containers. Forexample, a container can have a shape and size approximating that of acigarette pack or cigarette lighter. In some embodiments, a plurality ofgranules 10 can be packaged in an open or highly porous wrappingmaterial, (e.g., fabrics, paper or plastic films), with or withoutadditional smokeless tobacco product. In other embodiments, a pluralityof granules 10 can be packaged in a consumable package, (e.g., a pouchmade of a pair of edible film strips sealed or adhered together alongtheir edges). For example, the edible film used to produce a consumablepackage could be of the type described in U.S. Patent Publication No.2005/0089548, which is hereby incorporated by reference. A plurality ofdifferent types of granules 10 can be packaged together. In someembodiments, a first plurality of granules 10 having a first flavorprofile are packaged with a second plurality of granules 10 having asecond and different flavor profile. The first and second pluralities ofgranules can be visually differentiated by having different exteriorcolors. Different granule groups can be mixed or segregated.

Mixtures of granules, with or without other smokeless tobaccocompositions or other ingredients, can be molded, extruded, pressed, orotherwise formed into shaped smokeless tobacco pieces. In someembodiments, mixtures of granules, with or without other smokelesstobacco compositions or other ingredients, can be compressed to form atablet or disc. A tablet could then be packaged and/or dispensed in adispenser that includes stacked tablets and individually pushes out onetablet at a time upon activation of a dispensing mechanism. For example,granules 10 can be included in a non-dissolvable tobacco tablet or discwhere the granules 10 are dispersed within a matrix of non-dissolvablesmokeless tobacco material. A smokeless tobacco tablet or disc can alsobe made entirely of granules 10 pressed together. In other embodiments,a tablet could include a granule 10 layer on one side and a smoothtexture of another smokeless tobacco product on the reverse side toprovide a texture interplay Granules 10 can also be pressed into a baror stick shape. Pluralities of granules can also be pressed intoirregular cluster shapes. In some embodiments, clusters of granules 10can include a lipid coating (e.g., steric acid). Granules 10 can also bepressed into a flexible tape, which can be rolled up for distribution.The granules can also be molded around preformed items, such astoothpicks, pretzel sticks, other small cylinder shapes, or a flexiblecarrier. For example, granules 10 can be molded into pearl-like beads ona string to form a tobacco granule necklace.

Granules 10 can also include outer coatings that can give the granules10 desired bulk properties. For example, the outer coating can include asticky coating that allows an adult tobacco consumer to pinch aplurality of granules 10 together for consumption. In other embodiments,granules 10 can include an outer coating that inhibits bonding betweengranules 10, such that the granules 10 will easily flow. In otherembodiments, the materials used for the granules 10 can be selected toimpart a desired compressibility giving a desired mouth feel. Forexample, in some embodiments, the granules 10 can have a compressibilityapproximating that of a tapioca ball. In other embodiments, the granulescan be incompressible and designed to be crunched in an adult tobaccoconsumer's mouth.

Granules 10 can also be included with non-tobacco products. For example,granules 10 can be combined with a chewable gum to provide taste and/ortexture to the gum. In some embodiments, the gum can include additionalsmokeless tobacco products. In other embodiments, granules 10 can bepackaged along with a preformed object that can be dipped into a sectionof the packaging having granules 10 to coat the preformed object withgranules 10 for consumption. The preformed object can be made of anumber of consumable or non-consumable materials. For example, thepreformed object can be a lipid soft tab or a pressed sugar stick. Insome embodiments, the preformed object can include other smokelesstobacco products. In other embodiments, granules 10 can be includedwithin crystallized confectionaries, such as crystallized maple syrup.

IV. Granule Formation

The lipid mixture is formed into beads using a bead making machine(e.g., the Fuji Paudal Co. Ltd: Multi-Granulator, Model MC-55 andBenchtop Marumerizer Model #QJ-230T-1). The mixture includesmicrocrystalline cellulose (MCC), lipid, and water. The mixture can alsoinclude tobacco powder, sweeteners, flavorants, and other additives. Thetobacco powder can have an average size of about 35 microns. The beadsare then encapsulated with a coating. The encapsulation process may beany encapsulation process known in the art, including spray chilling,spray drying, spinning disk, coacervation, or some form of fluid bedprocess. Examples of encapsulation processes are described in U.S. Pat.Nos. 3,913,847; 6,153,236; 6,251,478; 6,312,741; 6,616,954; 6,673,383;6,797,291; and 6,835,397; the specifications, drawings and completedisclosures of which are incorporated herein by specific reference forall purposes. For example, the lipid cores can be coated using afluidized bed reactor to coat the lipid cores.

The resulting lipid granules can be mixed with various blends of tobaccoproduct. Liquid flavorants or sweeteners also may be used in the blend.Coatings on the lipid core can reduce adhesion between the lipidgranules. The coating can also stabilize the dimensions of the granules.One or more coatings can have a higher melting temperature than thelipid core. In one exemplary embodiment, the melting point of the one ormore coatings is 135.degree. F., or above. The granules can be stable inthe pH, high moisture, and high salt environment formed while in contactwith the tobacco product (or other product with moisture content) duringstorage, yet releases the flavor over time when the product is used.

Prophetic Example

Tobacco can be aged, fermented, pre-conditioned, cased, and milled toproduce particles with an average diameter of about 3 mm. Lipid beadscan be formed by adding a mixture of Encore 100 Palm Kernel oil (fromCargill); Avicel MCC PH-101; and water. Tobacco powder can also beadded. The lipid beads can be coated using a GXR30 system from VectorCorporation, which is capable of drying, coating, granulating and powderlayering. The tobacco particles can be fed to the GXR30 system fromVector Corporation using a screw powder-feeding apparatus. A coatingbinder, along with flavorants, sweeteners, and salts, can be sprayed asa binding solution into the GXR30 system. In some embodiments, thebinder can be MCC from FMC Biopolymer. The system can mix a tobaccopowder with the binding solution at a ratio of 1:1.3 tobaccopowder-to-binding solution. The coated lipid beads can have a coatingthickness of between 0.1 and 5.0 mm. The coated lipid bead can have anoven volatiles content of between 5 weight percent and 55 weightpercent. The coated lipid beads, in some embodiments, have between 5weight percent and 50 weight percent of tobacco (on a dry weight basis).

V. Other Embodiments

It is to be understood that, while the invention has been describedherein in conjunction with a number of different aspects, the foregoingdescription of the various aspects is intended to illustrate and notlimit the scope of the invention, which is defined by the scope of theappended claims. For example, a non-tobacco lipid bead could be made fortobacco and/or non-tobacco products. A non-tobacco lipid bead could havenon-tobacco actives in the lipid core and/or in one or more of thelayers. For example, a non-tobacco active could be caffeine. Otheraspects, advantages, and modifications are within the scope of thefollowing claims.

A number of embodiments have been described. Nevertheless, it will beunderstood that various modifications may be made without departing fromthe spirit and scope of this disclosure. For example, some smokelesstobacco products can include granules having a rapid release bindingagent that can be used in the outer layer for immediate satisfaction,then a slow release agent in the intermediate layers for sustainedflavor, and a lipid core for a final textural sensation. Still othersmokeless tobacco products can include combinations of granules havingdifferent flavorant, flavor release, and disintegration properties.Accordingly, other embodiments are within the scope of the followingclaims.

1. (canceled)
 2. A caffeinated granule product comprising: a pluralityof granules, each of the plurality of granules including, a coreincluding, a lipid caffeine, and a first binder, and a first layersurrounding the core, the first layer including a second binder.
 3. Thecaffeinated granule product of claim 2, wherein each of the plurality ofgranules further comprises: a second layer.
 4. The caffeinated granuleproduct of claim 3, wherein a composition of the first layer and acomposition of the second layer are different.
 5. The caffeinatedgranule product of claim 2, wherein the second binder is different fromthe first binder.
 6. The caffeinated granule product of claim 2, whereinthe first layer further comprises: a flavorant.
 7. The caffeinatedgranule product of claim 6, wherein the flavorant includes licorice,wintergreen, cherry and berry type flavorants, Drambuie, bourbon,scotch, whiskey, spearmint, peppermint, lavender, cinnamon, cardamon,apium graveolens, clove, cascarilla, nutmeg, sandalwood, bergamot,geranium, honey essence, rose oil, vanilla, lemon oil, orange oil,Japanese mint, cassia, caraway, cognac, jasmine, chamomile, menthol,ylang-ylang, sage, fennel, piment, ginger, anise, coriander, coffee,mint oils from a species of the genus Mentha, or any combinationthereof.
 8. The caffeinated granule product of product of claim 2,wherein the caffeinated granule product includes a flavor profile havingtwo different flavors, each of the two different flavors beingconfigured to have a peak flavor intensity being perceptible atdifferent times during consumption in a standardized sensory evaluation.9. The caffeinated granule product of claim 2, wherein each of theplurality of granules is spherical.
 10. The caffeinated granule productof claim 2, wherein the plurality of granules have an oven volatilescontent ranging from 5 weight percent to 55 weight percent.
 11. Thecaffeinated granule product of claim 2, wherein the core has a ratio oflipid to binder between 1:1 and 1:5.
 12. The caffeinated granule productof claim 2, wherein the core is between 5 and 70 weight percent lipid.13. The caffeinated granule product of claim 2, wherein the core isbetween 30 and 95 weight percent binder.
 14. The caffeinated granuleproduct of claim 2, wherein the granule does not include tobacco.